Aug 10, 2023
XRF Soil Sample Preparation
- rund.tawfiq 1
- 1CBRC, KAUST
Protocol Citation: rund.tawfiq 2023. XRF Soil Sample Preparation. protocols.io https://dx.doi.org/10.17504/protocols.io.n2bvj384plk5/v1
License: This is an open access protocol distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited
Protocol status: Working
We use this protocol and it's working
Created: August 10, 2023
Last Modified: August 10, 2023
Protocol Integer ID: 86315
Keywords: xrf soil sample preparation, xrf soil sample preparation this protocol, dry soil sample, soil sample, wet soil sample, accurate analysis of soil sample, accuracy of xrf analysis, xrf analysis, inorganic chemical analysis, understanding elemental composition, subsequent xrf analysis, elemental composition, potential interference with subsequent xrf analysis, proper grinding, xrf, elemental component, fluorescence, sample, proper preparation
Abstract
This protocol outlines a procedure for the preparation of both wet and dry soil samples for X-ray Fluorescence (XRF) inorganic chemical analysis. The accurate analysis of soil samples is essential for understanding elemental composition and its implications for various environmental studies. Proper preparation ensures reliable and reproducible results.
For wet soil samples, the protocol encompasses drying to remove excess moisture, preventing potential interference with subsequent XRF analysis.
For wet and dry soil samples, the protocol outlines grinding to ensure homogeneity and fine particle size. Proper grinding enhances the accuracy of XRF analysis by promoting even distribution and facilitating the release of elemental components.
Troubleshooting
Weigh ~500 mg of soil
30s
Dry Soil1 step
Dry soil is loose and crumbly to the touch and doesn't hold its shape when squeezed.
Grind with a mortar and pestle until the soil turns to powder (1-2 mins)