License: This is an open access collection distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited
Protocol status: Working
We use this collection and it's working
Created: May 29, 2025
Last Modified: July 29, 2025
Collection Integer ID: 219119
Keywords: advanced nmr materials ssnmr data acquisition protocol, nan materials ssnmr data acquisition protocols collection, part of the nan materials ssnmr knowledgebase, nan materials ssnmr knowledgebase, nmr, limited nmr expertise, state nmr, users with limited nmr expertise, links to the nan data browser, nan data browser, such as the quantitative bloch decay, common research questions in materials science, protocol, materials science, quantitative bloch decay, first batch of protocol, pulse program
Funders Acknowledgements:
National Science Foundation
Grant ID: 1946970
Abstract
The NAN Materials SSNMR Data Acquisition Protocols collection is part of the NAN Materials SSNMR Knowledgebase; a collection of resources, training and educational material, pulse programs and parameter sets, calibration procedures, sample data sets, and protocols designed to enable users with limited NMR expertise to design experiments, collect, and analyze NMR to address common research questions in materials science or chemistry using solid-state NMR. This collection includes the first batch of protocols, including both fundamental experiments (such as the quantitative Bloch decay or CPMAS) and advanced experiments (including D-HMQC and RESPDOR).
Each protocol contains links to the NAN Data Browser, where the relevant pulse program, pulse program files, and example data can be found.
Guidelines
These protocols have been successfully tested at NMRFAM, but are still under beta testing conditions. Use care when implementing them at a local facility, and consult with a local NMR expert when in doubt. Feedback is appreciated.
Safety warnings
While the protocols warn when there is a risk of damage to the NMR probe by using high power, the associated pulse programs do not have safety interlocks; always be cautious of the power level being applied to the probe.
Before start
To access the pulse programs associated with these protocols, visit the NAN data browser at usnan.nmrhub.org and navigate to the appropriate Knowledgebase entry.
